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Temperature Gradient Bar
Minimum Film Forming Temperature Bar
MFFTB


     

Example Applications

Minimum film forming temperature determination of:

· PAINTS
· ADHESIVES
· Latexes and emulsions
· Polymers

Failure temperature of grease-resistant paper:

· Food PACKAGING

Melt point of WAXES:

· Thermal transfer ribbons

Temperature optimisation:

· Confectionary (e.g. CHOCOLATE) processing
· EPOXY RESIN cure

This instrument was originally designed for the paint industry (hence name) but now has many other applications outside the paint industry where an accurate temperature gradient plate is required such as foods, cosmetics, confectionery, wrapping papers, adhesives, etc.

Minimum Film Forming Temperature (MFFT)

Definition

The lowest temperature at which a water-borne latex, emulsion, or adhesive, will uniformly coalesce when laid on a substrate as a thin film. The MFFT is related to the glass transition temperature, Tg, but is not identical.

Determination

The standard test for determining minimum film forming temperature involves using a MFFT Bar, as specified by such standards as ISO 2115 and ASTM D 2354. The design of the Rhopoint™ instrument is based directly on this standard. (Grooved platen for DIN 53787)

System

The Rhopoint™ Temperature Gradient Bar is a complete system, and the purchase of additional accessories is not required, provided that it is operated within the specifications. Fully integrated components include:

· Hinged perspex cover for thermal insulation and visual inspection
· Peltier cooling cells for sub-ambient temperatures
· Air drying system with re-usable desiccant
· Wet film cube applicator

Running

· The desired temperature program is selected and the instrument allowed to reach thermal equilibrium.
· Tracks of wet test material are applied to the platen using a cube applicator, and the hinged perspex cover is closed.
· Once the test material has dried, the process boundary or minimum film forming temperature is visually apparent, and can be pinpointed against ten temperature sensors using a moveable cursor.

Failure Temperature of Grease Resistant Paper

Definition

The minimum temperature at which a grease-resistant paper is wetted by fats or oils.

Determination

Failure temperature can be determined by laying sample strips of paper on the platen, using a small amount of adhesive, if necessary, and applying along it a quantity of the material to be contained. Within minutes, dark spots will appear in the paper where wetting has occurred. The lowest temperature at which 'spotting' occurs gives the result.

Melt Point of Waxes

Definition

The minimum temperature at which a dried waterborne wax, such as that used on thermal transfer printing ribbons, will start to exhibit liquid properties.

Determination

The wax suspension is applied in a track along the platen using a cube applicator. Drying occurs very quickly, and the melt point is given by the lowest temperature at which a clear fingerprint impression is left under the weight of the hand.

Temperature Optimisation

Definition

Conditions defining optimum temperatures at which other processes occur, such as extent of epoxy resin cure or separation of chocolate components, may be decided by the user according to production requirements.

Determination

Tracks of any type of liquid test material can easily and reproducibly be applied to the instrument platen using the cube applicator supplied. The visual or physical boundary temperature above or below which a critical process will occur can be easily pinpointed and accurately read.

Design

· The temperature bar consists of a nickel plated copper platen with an electronically imposed temperature gradient. Ten equispaced sensors beneath the surface provide instantaneous temperature measurement along the bar. A roving probe allows direct readings at any point, if required.
· Purge gas is integrally dried, and flows over the platen via a sintered distribution block. The hinged perspex cover provides thermal and atmospheric insulation whilst allowing constant visual inspection of an experiment.
· A cursor simplifies location of the exact temperature of result.

Standard Features

Two models of the MFFTB are available:

· MFFT-60: The standard model, which can operate over SIX different temperature ranges (1 - 6 in the table).
· MFFT-90: An extended range model, which can operate over NINE different temperature ranges (1 - 9 in the table).

Range
1
2
3
4
5
6
7
8
9
Cool end (°C)
-5
0
5
15
23
33
43
53
63
Warm end (°C)
13
18
23
33
50
60
70
80
90

Options

Copper platen (without nickel plating)No air processor fittedGrooved platen (for MFFT determination according to DIN 53787)

Specifications

Dimensions (l x w x h) : 550 x 610 x 350 mm
Platen dimensions (l x w) : 483 x 235 mm
Weight : 38 kg
Mains : 110 - 120 or 220 - 240 V AC
Air : 4l min-1 @ 100 psig
Water : Mains pressure; gravity drain; inlet temperature less than or equal to 20 °C